http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CA-1241659-A

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D249-20
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D249-20
filingDate 1985-04-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1988-09-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7e41061a52a178a49cbba614ac8675dc
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_38dec640fd2acd2173dee49b46f28528
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_65f41f290a7c4d17a7a92b9ebd34f781
publicationDate 1988-09-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CA-1241659-A
titleOfInvention Method for producing a 2-phenylbenzotriazole
abstract ABSTRACT OF THE DISCLOSURE: A method for producing a 2-phenylbenzotriazole useful as an ultraviolet absorber and represented by the general formula (III), (III) wherein R1 represents a hydrogen or chlorine atom, or a C1-C4 lower alkyl or lower alkoxy, carboxy or sulfonic acid group, R2 represents a hydrogen or chlorine atom, or a C1-C4 lower alkyl or lower alkoxy group, and R3, R4 and R5 each represent a hydrogen or chlorine atom, or a C1-C12 alkyl, phenyl, C1-C8 alkyl group-substituted phenyl, phenyl-C1-C8 alkyl, hydroxy, phenoxy or C1-C4 alkoxy group, which comprises reducing a 2-phenylbenzotriazol-N-oxide represented by the general formula (II), (II) wherein R1, R2, R3, R4 and R5 represent the same meanings as described above, with one or more members selected from the group consisting of phosphorus, hypophosphorous acid and its salts in the presence of an alkali and a naphthoquinone in the absence or presence of a surface active agent, or comprises reducing an o-nitroazobenzene represented by the general formula (I), (I) wherein R1, R2, R3, R4 and R5 represent the same meanings as described above, with one or more members selected from the group consisting of phosphorus, hypophosphorous acid and its salts in the presence of an alkali and a naphthoquinone in the absence or presence of a surface active agent to obtain a 2-phenyl-benzotriazol-N-oxide represented by the general formula (II), (II) wherein R1, R2, R3, R4 and R5 represent the same meanings as described above, and reducing the resulting compound (II) with one or more members selected from the group consisting of phosphorus, hypophosphorous acid and its salts in the presence of an alkali and a naphthoquinone in the absence or presence of a surface active agent.
priorityDate 1984-04-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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