http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CA-1066302-A

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classificationCPCAdditional http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-10
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C63-26
filingDate 1976-04-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1979-11-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a6b8960b1cfbfa10ea651ad8b6662ebb
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_804c6a2eeeac79899682341454ba58d2
publicationDate 1979-11-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CA-1066302-A
titleOfInvention Process for making aromatic acids
abstract ABSTRACT OF THE DISCLOSURE A process for making an aromatic carboxylic acid of high purity by feeding an essentially equilibrium hydrolysis mixture of an aromatic nitrile to a reactive distillation column operated at a temperature of from about 200°C. to about 325°C. at autogenous pressure where the equilibrium mixture is subjected simultaneously to further hydrolysis and distillation of ammonia, removing water vapor and ammonia from the top of the column, subjecting remaining equilibrium hydrolysis mixture to further hydrolysis and distill-ation in a reboiler, returning vapor from the reboiler to the distillation column, removing an aqueous solution of product acid from the reboiler, cooling said separated solution, and separating acid product. In one embodiment of the invention the hydrolysis mixture is obtained by subjecting a nitrile from the ammoxidation of an alkyl aromatic compound to aqueous hydrolysis in a closed reactor at about 200°C to about 325°C. until an essentially complete equilibrium is obtained.
priorityDate 1976-04-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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