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publicationDate 2021-06-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber BR-112017017246-B1
titleOfInvention METHOD FOR CONTINUOUS PREPARATION OF APPARENT HIGH DENSITY METHIONE CRYSTAL
abstract METHOD FOR CONTINUOUS PREPARATION OF APPARENT HIGH DENSITY METHIONE CRYSTAL. The present invention relates to a method for the continuous preparation of high bulk density methionine crystals. The method process is as follows: a hydrolyzate, which is obtained from a reaction of 5-(β-methylthioethyl)hydantoin and a potassium carbonate solution, is mixed with an externally circulating material from a DTB neutralization crystallizer with a gas phase neutralization section; after the mixture is cooled, the mixture enters a liquid distributor from a neutralizing region at the top of the crystallizer; the mixture is sprayed into droplets or drops of liquid in carbon dioxide gas for the neutralization reaction and then naturally falls into a crystallization region at the bottom to be mixed with a material in the region; the mixture grows into small crystals in a system to form crystals with larger particle diameters and meanwhile new crystal nuclei are formed; in a settling region in the middle part of the crystallization region, crystals with larger particle diameters sink in a (...) collector.
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