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filingDate 2013-12-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8ba141600c096424ea2bd1478208fdf2
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publicationDate 2021-01-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber BR-112015014628-B1
titleOfInvention process for producing acetic acid, and method for separating or removing acetaldehyde
abstract process for producing acetic acid, and method for separating or removing acetaldehyde. a method is provided to effectively remove acetaldehyde and produce acetic acid in a stable manner. methanol and carbon monoxide are reacted continuously in a carbonylation reactor (1) in the presence of a catalyst system, the reaction mixture is continuously supplied to an expander (2), and a volatile phase (2a) containing acetic acid and iodide of methyl is produced the volatile phase (2a) is continuously supplied to a separation column (3) and separated at the top (3a) containing methyl iodide and acetaldehyde, and flow fraction (3b) containing acetic acid. the volatile phase (2a) and / or the upper part (3a) are cooled by first condensers (c1, c3) having a predetermined cooling temperature, the non-condensed gas component is additionally cooled by second condensers (c2, c4) and condenses do, the temperature is further lowered, and a concentrate in which acetaldehyde was concentrated to a high concentration is produced. the high concentration acetaldehyde concentrate is distilled through a distillation column (6), and the acetaldehyde is effectively removed.
priorityDate 2012-12-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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