http://rdf.ncbi.nlm.nih.gov/pubchem/patent/AU-2018100417-A4

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_342853f417bdfe26db108fac8073eb74
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C51-00
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C53-126
filingDate 2018-04-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2018-05-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1cb39cbdf0b5b1f5169a9df396687d74
publicationDate 2018-05-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber AU-2018100417-A4
titleOfInvention Raw materials of organic synthesis tridecanoic acid synthesis method
abstract Abstract Raw materials of organic synthesis tridecanoic acid synthesis method, comprises the following steps: 2 mol 2-bromotetradecanol, 4-6 mol dioctyl phthalate solution 5 were added to the reaction vessel, controlled the stirring speed at 150-180 rpm for 70-90 min and controlled solution temperature to 2-5 "C, added 3-4 mol titanium aluminium chloride, continued to react 130-160 min, added 700 ml sodium bromide solution, standing for 20-40 min, separated the oil layer, washed with m-chlorophenol solution, washed with formamide solution, recrystallizated in the methyl sulfide 10 solution, dehydrated with dehydration, got the finished product tridecanoic acid.
priorityDate 2017-04-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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