http://rdf.ncbi.nlm.nih.gov/pubchem/patent/AU-2018100417-A4
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_342853f417bdfe26db108fac8073eb74 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C51-00 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C53-126 |
filingDate | 2018-04-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2018-05-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1cb39cbdf0b5b1f5169a9df396687d74 |
publicationDate | 2018-05-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | AU-2018100417-A4 |
titleOfInvention | Raw materials of organic synthesis tridecanoic acid synthesis method |
abstract | Abstract Raw materials of organic synthesis tridecanoic acid synthesis method, comprises the following steps: 2 mol 2-bromotetradecanol, 4-6 mol dioctyl phthalate solution 5 were added to the reaction vessel, controlled the stirring speed at 150-180 rpm for 70-90 min and controlled solution temperature to 2-5 "C, added 3-4 mol titanium aluminium chloride, continued to react 130-160 min, added 700 ml sodium bromide solution, standing for 20-40 min, separated the oil layer, washed with m-chlorophenol solution, washed with formamide solution, recrystallizated in the methyl sulfide 10 solution, dehydrated with dehydration, got the finished product tridecanoic acid. |
priorityDate | 2017-04-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 34.